(S)-BinapRu(all)2; hydrogen in toluene T=25°C; P=53200 Torr; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
(+)-(S)-α-Np-BTM; 4-methoxybenzoic anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 35 p. 5887 - 5890
disodium hydrogenphosphate; hydrogen; palladium on activated charcoal in methanol T=100°C; P=760 Torr; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
