反应条件
1: 88 percent / AlCl3 / CH2Cl2 / 12 h / 25 °C 2: 90 percent / diethyl ether / 1.) 20 deg C, 10 h, 2.) reflux, 30 min 3: 90 percent / POCl3, Py / CH2Cl2 / 0 - 25 °C 4: K3Fe(CN)6, K2CO3, OsO4, (DHQD)2-PHAL, MeSO2NH2 / H2O; 2-methyl-propan-2-ol; toluene / 28 h / 0 °C 5: HCOONH4 / Pd-C / ethanol / 6 h / Heating 6: Jone's reagent / acetone / 8 h / 0 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 37, # 12 p. 1221 - 1227
