2,2'-联吡啶-6-硫醇合成路线 (共 4 条)
反应条件
NaHS monohydrate in N,N-dimethyl-formamide
参考文献
Pornsuriyasak, Papapida; Rath, Nigam P.; Demchenko, Alexei V.
Chemical Communications, 2008 , # 43 p. 5633 - 5635
反应条件
potassium hydroxide; sodium hydrogensulfide in N,N-dimethyl-formamide Heating;
参考文献
Wang, Qiang; Day, Peter; Griffiths, Jon-Paul; Nie, Hui; Wallis, John D.
New Journal of Chemistry, 2006 , vol. 30, # 12 p. 1790 - 1800
反应条件
1: 75 percent / m-chloroperbenzoic acid / CHCl3 / 13 h / Ambient temperature 2: 41 percent / POCl3 / 12 h / Heating 3: 80 percent / KSH / dimethylformamide / 4 h / Heating View Scheme
参考文献
Wang, Fen; Schwabacher, Alan W.
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4779 - 4782
反应条件
1: 41 percent / POCl3 / 12 h / Heating 2: 80 percent / KSH / dimethylformamide / 4 h / Heating View Scheme
参考文献
Wang, Fen; Schwabacher, Alan W.
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4779 - 4782