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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
间溴苯甲醚
合成路线
（共 423 条）
2398-37-0
间溴苯甲醚
→
反应条件
6933-49-9
2-甲氧基-9H-咔唑
反应条件
1: 81 percent / copper bronze, K2CO3 / 7 h / Heating 2: 61 percent / KOH / ethanol / 1.5 h / Heating 3: 2.6 mg / hexane / 8 h / Irradiation View Scheme
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Long, Anthony; Oliveira-Campos, Ana; Shannon, Patrick V. R.
Journal of Chemical Research, Miniprint, 1986 , # 8 p. 2645 - 2696
2398-37-0
间溴苯甲醚
→
反应条件
626-20-0
3-甲氧基苯乙烯
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in tetrahydrofuran; water T=85°C; Suzuki-Miyaura reaction; 22 h;
参考文献
Molander, Gary A.; Brown, Adam R.
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9681 - 9686
108-05-4
醋酸乙烯酯
+
2398-37-0
间溴苯甲醚
→
反应条件
626-20-0
3-甲氧基苯乙烯
反应条件
[2,2']bipyridinyl; tetra-n-butylammonium tetrafluoroborate; cobalt(II) dibromide in pyridine; acetonitrile T=20°C; Electrolysis;
参考文献
Gomes, Paulo; Gosmini, Corinne; Perichon, Jacques
Tetrahedron, 2003 , vol. 59, # 17 p. 2999 - 3002
2398-37-0
间溴苯甲醚
→
反应条件
768-70-7
3-乙炔基苯甲醚
反应条件
1: Et3N; CuI / Pd(PPh3)4 / Heating 2: K2CO3 / methanol / 20 °C View Scheme
参考文献
Musso, David L; Clarke, Morris J; Kelley, James L; Boswell, G Evan; Chen, Grace
Organic and biomolecular chemistry, 2003 , vol. 1, # 3 p. 498 - 506
2398-37-0
间溴苯甲醚
+
1066-54-2
三甲基乙炔基硅
→
反应条件
768-70-7
3-乙炔基苯甲醚
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=20 - 60°C; 12 h; Inert atmosphere;
参考文献
Guo, Rui; Li, Kang-Nan; Gong, Liu-Zhu
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6707 - 6712
2398-37-0
间溴苯甲醚
→
反应条件
52488-36-5
4-溴吲哚
反应条件
1.1: t-Bu2Zn(tmp)Li / tetrahydrofuran / -30 °C 2.1: boron tribromide / dichloromethane / -78 - 20 °C 2.2: 0 - 20 °C 3.1: sodium hydroxide / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere 3.2: 2 h / 20 °C / Inert atmosphere 4.1: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere 5.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / N,N-dimethyl-formamide / 3 h / 40 °C / Inert atmosphere 6.1: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 140 °C / Inert atmosphere View Scheme
参考文献
Guilarte, Veronica; Castroviejo, M. Pilar; Garcia-Garcia, Patricia; Fernandez-Rodriguez, Manuel A.; Sanz, Roberto
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3416 - 3437
2398-37-0
间溴苯甲醚
→
反应条件
621-27-2
3-正-丙基苯酚
反应条件
1: iodine; magnesium / tetrahydrofuran 2: boron tribromide / chloroform View Scheme
参考文献
Bouchoux, Guy; Sablier, Michel; Miyakoshi, Tetsuo; Honda, Takashi
Journal of Mass Spectrometry, 2012 , vol. 47, # 4 p. 539 - 546
2398-37-0
间溴苯甲醚
+
111-34-2
乙烯基正丁醚
→
反应条件
586-37-8
3'-甲氧基苯乙酮
反应条件
1: With meso-2,4-bis(diphenylphosphino)pentane; triethylamine; palladium diacetate in dimethyl sulfoxide T=115°C; Heck arylation; 36 h; 2: With hydrogenchloride in dimethyl sulfoxide T=20°C;
参考文献
Liu, Shifang; Berry, Neil; Thomson, Nick; Pettman, Alan; Hyder, Zeynab; Mo, Jun; Xiao, Jianliang
Journal of Organic Chemistry, 2006 , vol. 71, # 19 p. 7467 - 7470
2398-37-0
间溴苯甲醚
+
75-36-5
乙酰氯
→
反应条件
586-37-8
3'-甲氧基苯乙酮
反应条件
1: 3-methoxybromobenzene With trifluoroacetic acid; cobalt(II) dibromide; zinc; zinc dibromide in acetonitrile T=20°C; 2: acetyl chloride in acetonitrile T=20°C;
参考文献
Fillon, Hyacinthe; Gosmini, Corinne; Perichon, Jacques
Tetrahedron, 2003 , vol. 59, # 41 p. 8199 - 8202
2398-37-0
间溴苯甲醚
+
108-24-7
乙酸酐
→
反应条件
586-37-8
3'-甲氧基苯乙酮
反应条件
3-chloroprop-1-ene; cobalt(II) dibromide; zinc; trifluoroacetic acid in acetonitrile 0.5 h;
参考文献
Kazmierski, Igor; Bastienne, Mylene; Gosmini, Corinne; Paris, Jean-Marc; Perichon, Jacques
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 936 - 942
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