1: With n-butyllithium in tetrahydrofuran; hexane T=0°C; Flow reactor; 2: With 2-fluoro-3,3-dimethyl-2,3-dihydro-1,2-benzisothiazole-1,1-dioxide in tetrahydrofuran; hexane T=0°C; Flow reactor; Reagent/catalyst;
参考文献
Nagaki, Aiichiro; Uesugi, Yuki; Kim, Heejin; Yoshida, Jun-Ichi
Chemistry - An Asian Journal, 2013 , vol. 8, # 4 p. 705 - 708
1: 3-methoxybromobenzene With magnesium in tetrahydrofuran T=40°C; 2 h; 2: benzyl 2,6-dioxotetrahydro-2H-pyran-3-ylcarbamate in tetrahydrofuran T=-78°C; 4 h; 3: With citric acid in tetrahydrofuran T=-78 - 20°C; Title compound not separated from byproducts;
参考文献
Deguest, Geoffrey; Bischoff, Laurent; Fruit, Corinne; Marsais, Francis
Tetrahedron Asymmetry, 2006 , vol. 17, # 14 p. 2120 - 2125
magnesium; iodine in tetrahydrofuran T=20°C; Heating / reflux;
参考文献
Yoder, Claude H.; Agee, Tamara M.; Griffith, Allison K.; Schaeffer Jr., Charles D.; Carroll, Mary J.; Detoma, Alaina S.; Fleisher, Adam J.; Gettel, Cameron J.; Rheingold, Arnold L.
Organometallics, 2010 , vol. 29, # 3 p. 582 - 590
