Cornforth, John; Sierakowski, Andrew F.; Wallace Timothy W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2299 - 2316
1.1: n-BuLi / tetrahydrofuran / 1 h / -78 °C
1.2: tetrahydrofuran / 2 h / -78 - 20 °C
2.1: H2O2 / methanol / 0.5 h / 20 °C
3.1: LDA / tetrahydrofuran / 1.5 h / -78 °C
3.2: 76 percent / I2 / tetrahydrofuran / 1 h / -78 - 20 °C
4.1: 93 percent / BBr3 / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Gorobets, Evgueni; Wheatley, Bronwen M. M.; Hopkins, J. Matthew; McDonald, Robert; Keay, Brian A.
Tetrahedron Letters, 2005 , vol. 46, # 22 p. 3843 - 3846