甲基 6-甲氧基-2-萘乙酸酯合成路线 (共 27 条)
反应条件
hydrogenchloride; sulfuric acid; hydrogen sulfide; acetic acid in methanol; ethyl acetate
反应条件
sodium borohydride; hydrogen; palladium-on-barium sulfate; palladium in hydrogenchloride; diethyl ether; ethanol; chloroform; water; acetic acid; toluene
反应条件
AgBF4 in methanol; water; trimethyl orthoformate
参考文献
US5747505 A1, ;
US 5747505 A
反应条件
sulfuric acid 8 h; Heating;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 6 p. 1292 - 1298
反应条件
sulfuric acid Reflux;
参考文献
WO2010/129505 A2, ;
Page/Page column 37 ;
WO 2010/129505 A2
反应条件
sulfuric acid in methanol 6 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 428 - 439
反应条件
1: 91.7 percent / NaBH4 / methanol; H2O / 2 h / Ambient temperature 2: gaseous HCl / benzene / 2 h / 60 °C 3: dimethylformamide / 3 h / Ambient temperature 4: 64.1 percent / cc. H2SO4 / methanol / 6 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 428 - 439
反应条件
perchloric acid; thallium(III) nitrate Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 26, # 5 p. 700 - 714
反应条件
1: 1,1,2,2-tetramethylethylene; potassium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 0.73 h / 20 °C 2: sulfuric acid / 2 h / |Reflux View Scheme
参考文献
ACS Medicinal Chemistry Letters, , vol. 3, # 9 p. 759 - 763
反应条件
1: 70.2 percent / Mg / tetrahydrofuran / rt, 1 h, reflux 6 h 2: 91.7 percent / NaBH4 / methanol; H2O / 2 h / Ambient temperature 3: gaseous HCl / benzene / 2 h / 60 °C 4: dimethylformamide / 3 h / Ambient temperature 5: 64.1 percent / cc. H2SO4 / methanol / 6 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 428 - 439