2-(6-甲氧基-2-萘基)丙酸合成路线 (共 130 条)
反应条件
potassium hydroxide; polyethylene glycol (PEG-400); potassium cyanide; nickel cyanide; cobalt(II) chloride in toluene T=90°C; P=760 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 32, # 15 p. 1769 - 1770
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite in water; acetonitrile T=20°C; 21 h; aq. phosphate buffer;
参考文献
Galletti, Paola; Pori, Matteo; Giacomini, Daria
Synlett, 2010 , # 17 p. 2644 - 2648
反应条件
sodium hydroxide; iodine in methanol
参考文献
Zambon S.p.A.
Patent: US4501913 A1, 1985 ;
反应条件
formic acid; palladium on activated charcoal in hexane 6 h; Ambient temperature; Yield given;
参考文献
Tetrahedron, , vol. 49, # 37 p. 8433 - 8440
反应条件
toluene-4-sulfonic acid; triphenylphosphine; lithium chloride; Pd-support in water; butanone T=115°C; Carbonylation; P=40503.2 Torr; 24 h; Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 12 p. 1067 - 1068
反应条件
TPPTS; toluene-4-sulfonic acid; lithium chloride; 2-PyCOO-Pd-OTs in water; toluene T=115°C; Carbonylation; P=40504.1 Torr; 12 h; Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 14 p. 1239 - 1240
反应条件
cobalt(II)salen; tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide T=5°C; P=760 Torr; Electrochemical reaction;
参考文献
Damodar; Krishna Mohan; Khaja Lateef; Jayarama Reddy
Synthetic Communications, 2005 , vol. 35, # 9 p. 1143 - 1150
参考文献
Montedison S.p.A.
Patent: US4536595 A1, 1985 ;
反应条件
2,2'-azo-bisisobutyronitrile in benzene T=65 - 70°C; 3 h;
参考文献
Perchyonok, V. Tamara; Ryan, Sarah J.; Langford, Steven J.; Hearn, Milton T.; Tuck, Kellie L.
Synlett, 2008 , # 8 p. 1233 - 1235
反应条件
1: t-BuOK / hexane / 0.5 h / 20 °C 2: H2, HClO4 / 10 percent Pd/C / hexane / 20 °C View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 24, # 2 p. 165 - 167