1,3-二氯-1,1,3,3,-四甲基二硅氧烷合成路线 （共 57 条）
反应条件
CuI; triphenylphosphine; (PPh3)2PdCl2 in triethylamine; toluene
参考文献
The Government of the United States of America, as represented by the Secretary of the Navy
Patent: US2011/306744 A1, 2011 ;
参考文献
Bulkowski,J.E. et al.
Journal of Organometallic Chemistry, 1975 , vol. 101, p. 267 - 277
参考文献
Forbes, Malcolm D. E.; Patton, Jasson T.; Myers, Tanya L.; Maynard, Heather D.; Smith, Dennis W.; et al.
Journal of the American Chemical Society, 1992 , vol. 114, # 27 p. 10978 - 10980
反应条件
1: para-bromotoluene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: 1,3-dichloro-1,1,3,3-tetramethyldisiloxane in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphere;
参考文献
Boehner, Christine M.; Frye, Elizabeth C.; O'Connell, Kieron M. G.; Galloway, Warren R. J. D.; Sore, Hannah F.; Dominguez, Patricia Garcia; Norton, David; Hulcoop, David G.; Owen, Martin; Turner, Gillian; Crawford, Claire; Horsley, Helen; Spring, David R.
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13230 - 13239
反应条件
pyridine in diethyl ether 2 h; Heating;
参考文献
Kaeppler, K.; Scheim, U.; Ruehlmann, K.; Porzel, A.
Journal of Organometallic Chemistry, 1992 , vol. 441, # 1 p. 15 - 25
反应条件
in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Graeper, Jens; Fischer, R. Dieter; Paolucci, Gino
Journal of Organometallic Chemistry, 1994 , vol. 471, # 1-2 p. 87 - 96
参考文献
Wacker-Chemie GmbH
Patent: US6284907 B1, 2001 ;
反应条件
water 1.) petroleum ether, ether, -78 deg C, 3 h; Multistep reaction;
参考文献
Kazoura, Samih Amine; Weber, Wolliam P.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 2 p. 149 - 156
反应条件
water 1.) ether, pentane, -78 deg C, 50 min, 2.) ether, pentane, THF, -78 deg C, 20 min; Multistep reaction;
参考文献
Kazoura, Samih Amine; Weber, Wolliam P.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 2 p. 149 - 156
反应条件
water 1.) ether, hexane, -78 deg C, 1.5 h; Multistep reaction;
参考文献
Kazoura, Samih Amine; Weber, Wolliam P.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 2 p. 149 - 156
