3-甲氧基-2-硝基-6-甲基吡啶合成路线 （共 9 条）
反应条件
potassium carbonate in dimethyl sulfoxide T=20°C;
参考文献
Wyeth
Patent: US2006/173049 A1, 2006 ;
Location in patent: Page/Page column 23-24 ;
US 20060173049 A1
反应条件
in methanol; diethyl ether; dichloromethane
参考文献
Boehringer Ingelheim (Canada) Ltd.
Patent: US2003/236251 A1, 2003 ;
Location in patent: Page 23 ;
参考文献
Kureha Kagaku Kogyo K.K.
Patent: US6610853 B1, 2003 ;
反应条件
1: 86 percent / conc. H2SO4, fuming HNO3 / 2 h / 20 °C 2: 67 percent / K2CO3 / acetone / Heating View Scheme
参考文献
Heterocycles, , vol. 38, # 3 p. 529 - 540
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 19, # 23 p. 6507 - 6514
反应条件
ammonia in diethyl ether; water; magnesium sulfate
反应条件
1: With potassium permanganate; water T=75°C; 18 h; 2: With hydrogenchloride; water T=0°C;
参考文献
Cheng, Cliff C.; Shipps Jr., Gerald W.; Yang, Zhiwei; Sun, Binyuan; Kawahata, Noriyuki; Soucy, Kyle A.; Soriano, Aileen; Orth, Peter; Xiao, Li; Mann, Paul; Black, Todd
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 23 p. 6507 - 6514
参考文献
Kureha Kagaku Kogyo K.K.
Patent: US6610853 B1, 2003 ;
反应条件
hydrogen; palladium on activated carbon in ethanol
2 h;
参考文献
Kyorin Pharmaceutical Co., Ltd.
Patent: EP2168960 A1, 2010 ;
Location in patent: Page/Page column 70 ;
