3-烯丙基-2-羟基苯甲醛合成路线 （共 17 条）
反应条件
hydrogenchloride in ethanol
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Patent: WO2008/134474 A2, 2008 ;
Location in patent: Page/Page column 68 ;
反应条件
1: 77 percent / K2CO3 / acetone / 2 h / 60 °C 2: 57 percent / [RuClH(CO)(PPh3)3] / CH2Cl2 / 14 h / 65 °C 3: 70 percent / ((Mes)2C3H5N2)Cl2Ru=CHPh / toluene / 3 h / 90 °C View Scheme
参考文献
Van Otterlo, Willem A.L.; Morgans, Garreth L.; Madeley, Lee G.; Kuzvidza, Samuel; Moleele, Simon S.; Thornton, Natalie; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 32 p. 7746 - 7755
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 3 h;
参考文献
Peterson, Quinn P.; Hsu, Danny C.; Goode, David R.; Novotny, Chris J.; Totten, Ryan K.; Hergenrother, Paul J.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 18 p. 5721 - 5731
反应条件
1: piperidine
2: aq.-ethanolic KOH-solution
View Scheme
参考文献
Buu-Hoi et al.
Bulletin de la Societe Chimique de France, 1947 , p. 128,135
反应条件
sodium hydroxide
Erwaermen des Reaktionsprodukts mit wss. Salzsaeure;
参考文献
Endo Prod. Inc.
Patent: US2683720 , 1949 ;
反应条件
4,4'-diphenylsulfide; 5 palladium on charcoal; hydrogen in ethyl acetate
T=20°C;
参考文献
HERGENROTHER, Paul J.; ROTH, Howard Steven; THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Patent: WO2014/22858 A1, 2014 ;
Location in patent: Page/Page column 46 ;
反应条件
potassium carbonate in methanol; water
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Patent: WO2008/134474 A2, 2008 ;
Location in patent: Page/Page column 70 ;
