1: With hydrogenchloride; sodium nitrite in water T=5 - 15°C; 0.75 h; 2: With hydrogenchloride; aminosulfonic acid; CuCl2*2H2O in water T=55 - 62°C; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/114589 A1, 2009 ;
Location in patent: Page/Page column 13-14 ;
1: With hydrogenchloride; anhydrous iron chloride; chlorine; sodium nitrite in water T=-8 - 20°C; 2: With hydrogenchloride; copper(l) chloride in water T=60 - 70°C;
trichlorophosphate in N,N-dimethyl-formamide T=95°C; 12 h;
参考文献
Lai, Long-Li; Lin, Pen-Yuan; Wang, Jy-Shih; Hwu, Jih Ru; Shiao, Min-Jen; Tsay, Shwu-Chen
Journal of Chemical Research - Part S, 1996 , # 4 p. 194 - 195
Lai, Long-Li; Lin, Pen-Yuan; Wang, Jy-Shih; Hwu, Jih Ru; Shiao, Min-Jen; Tsay, Shwu-Chen
Journal of Chemical Research - Part S, 1996 , # 4 p. 194 - 195
