2,3,5,6-四氯吡啶合成路线 (共 54 条)
反应条件
isopropyl-benzene; copper in N,N-dimethyl-formamide T=150°C; 1 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
thionyl chloride; copper(l) chloride T=150°C; P=4560.31 Torr; 5 h;
参考文献
Organic Process Research and Development, , vol. 7, # 3 p. 329 - 333
反应条件
copper in N,N-dimethyl-formamide T=150°C; 20 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
1: copper(I) iodide / tetrahydrofuran 2: 9 percent / dimethylformamide / 0.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
copper(l) chloride T=120 - 150°C; P=1140.08 - 4560.31 Torr; 6 h; Overall yield = 182 g;
参考文献
Organic Process Research and Development, , vol. 7, # 3 p. 329 - 333
反应条件
copper(l) chloride T=150°C; P=4560.31 Torr; 5 h;
参考文献
Organic Process Research and Development, , vol. 7, # 3 p. 329 - 333
反应条件
sodium hydroxide; 1,2,2-trichloro-1,1,2-trichloro-ethane; tetrabutylammomium bromide T=50°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 45, # 26 p. 5061 - 5063
参考文献
Journal of the Chemical Society, , vol. 71, p. 1082
Journal of the Chemical Society, , vol. 73, p. 441
反应条件
copper in N,N-dimethyl-formamide T=150°C; 20 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687