2,3,5,6-四氯吡啶合成路线 （共 54 条）
反应条件
1: 16 percent / copper bronze, cumene / dimethylformamide / 1 h / 150 °C 2: 3 percent Chromat. / copper bronze / dimethylformamide / 20 h / 150 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
phosphorus pentachloride T=210 - 220°C;
参考文献
Journal of the Chemical Society, , vol. 73, p. 437
反应条件
phosphorus pentachloride; trichlorophosphate T=180°C;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 70, p. 182,190
反应条件
1: copper bronze / dimethylformamide / 150 °C 2: 3 percent Chromat. / copper bronze / dimethylformamide / 20 h / 150 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
1: 1 percent / p-xylene, benzoyl chloride / dimethylformamide / 23 h / Heating 2: 3 percent Chromat. / copper bronze / dimethylformamide / 20 h / 150 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
in diethyl ether 71 h; Irradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 648 - 656
反应条件
para-xylene; benzoyl chloride in N,N-dimethyl-formamide 23 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
in N,N-dimethyl-formamide Hg cathode, -1.40 V (S.C.E.), Et4NBF4;
参考文献
Tetrahedron, , vol. 37, p. 591 - 595
反应条件
1: water; hydrochloric acid / 160 °C / Unter Druck 2: hydrogen peroxide; water; hydrochloric acid 3: phosphorus (V)-chloride; phosphoryl chloride / 180 °C View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 70, p. 182,190
反应条件
ammonium chloride; methanephosphonic acid dimethyl ester; zinc in water T=85 - 90°C; other ammonium salts; other methylphosphonates/phosphates; Product distribution;
参考文献
Journal of Heterocyclic Chemistry, , vol. 17, p. 493 - 496
