With chloro-trimethyl-silane; sodium iodide in acetonitrile T=25°C; 3 h;
参考文献
Tsuboi, Sadao; Wu, Xue Han; Maeda, Seiji; Ono, Shinichiro; Kuroda, Akihisha; et al. Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 3 p. 1103 - 1108
Multi-step reaction with 2 steps 1: 1.) Mg / 1.) THF, 2 h, 2.) THF, -15 deg C, 2 h2: 54 percent / Me3SiCl, NaI / acetonitrile / 3 h / 25 °C
参考文献
Tsuboi, Sadao; Wu, Xue Han; Maeda, Seiji; Ono, Shinichiro; Kuroda, Akihisha; et al. Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 3 p. 1103 - 1108
