3-硝基-1-氧代吡啶-1-鎓合成路线 (共 5 条)
反应条件
Potassium peroxomonosulfate; sodium hydrogencarbonate in methanol; water T=47°C; 20 h; Inert atmosphere;
参考文献
Vamos, Mitchell; Cosford, Nicholas D. P.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2274 - 2280
反应条件
selenium(IV) oxide in 1,4-dioxane 7 h; Heating;
参考文献
Achremowicz, Lucjan
Tetrahedron Letters, 1980 , vol. 21, p. 2433 - 2434
反应条件
trichlorophosphate T=110°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Yamanaka, Hiroshi; Araki, Tomio; Sakamoto, Takao
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, p. 2244 - 2247
反应条件
trichlorophosphate T=110°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Yamanaka, Hiroshi; Araki, Tomio; Sakamoto, Takao
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, p. 2244 - 2247
反应条件
trimethylsilyl cyanide; triethylamine in acetonitrile 24 h; Heating;
参考文献
Sakamoto, Takao; Kaneda, Soh-ichi; Nishimura, Sumiko; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 2 p. 565 - 571