2-(4-甲基苯基)-1,3-二氧戊环合成路线 （共 22 条）
反应条件
polyaniline-sulfate salt; water 0.5 h; Heating;
参考文献
Synlett, , # 12 p. 1793 - 1796
反应条件
in dichloromethane T=50°C; 0.0833333 h; Microwave irradiationSealed tube;
参考文献
Arkivoc, , vol. 2013, # 3 p. 98 - 108
反应条件
tungsten hexachloride in dichloromethane
T=0 - 5°C; 0.25 h;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Karimi, Babak
Synlett, 1998 , # 7 p. 739 - 740
反应条件
1: 90 percent / solid silica chloride / CH2Cl2 / 0.33 h / 20 °C
2: 96 percent / solid silica chloride / acetonitrile / 20 °C
3: 95 percent / solid silica chloride / CHCl3 / 0.25 h / 20 °C
View Scheme
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
triethylsilane; iodine in acetonitrile
5 h; Inert atmosphereReflux; chemoselective reaction;
参考文献
Zhang, Xue-Lin; Yu, Pan; Wu, Yong-Wei; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2014 , vol. 38, # 5 p. 261 - 264
反应条件
2,2'-azo-bisisobutyronitrile; tribromo methane in benzene
5 h; Heating;
参考文献
Hai-Xia, Lin; Liang-Heng, Xu; Nai-Ju, Huang
Synthetic Communications, 1997 , vol. 27, # 2 p. 303 - 306
反应条件
tin(II) trifluoromethanesulfonate; dimethyl tert-butyl silane in acetonitrile
T=-20°C;
参考文献
Suzuki, Takeshi; Oriyama, Takeshi
Synthetic Communications, 1999 , vol. 29, # 8 p. 1263 - 1269
反应条件
[MoCl5] in dichloromethane
T=20°C; 36 h;
参考文献
Firouzabadi; Karimi
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 175, p. 207 - 216
反应条件
acetyl chloride in methanol
0.5 h; RefluxGreen chemistry; TemperatureTime; chemoselective reaction;
参考文献
Yu, Hai-Feng
Synthetic Communications, 2013 , vol. 43, # 9 p. 1280 - 1286
反应条件
1: 90 percent / solid silica chloride / CH2Cl2 / 0.33 h / 20 °C
2: 96 percent / solid silica chloride / acetonitrile / 20 °C
3: 96 percent / solid silica chloride / CHCl3 / 0.25 h / 20 °C
View Scheme
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
