2-(4-硝基苯基)-1,3-二氧戊环合成路线 (共 34 条)
反应条件
hydrogen; platinum(IV) oxide in tetrahydrofuran
参考文献
Riddle, Justin A.; Jiang, Xuan; Huffman, John; Lee, Dongwhan
Angewandte Chemie - International Edition, 2007 , vol. 46, # 37 p. 7019 - 7022
反应条件
toluene-4-sulfonic acid; trimethyl orthoformate; PtO2 in tetrahydrofuran; H2; water; ethylene glycol; toluene
参考文献
The Standard Oil Company
Patent: US4740611 A1, 1988 ;
反应条件
hydroxide solution; oxygen in water Irradiationvarious pH; Quantum yieldMechanism;
参考文献
Wan, Peter
Tetrahedron Letters, 1985 , vol. 26, # 20 p. 2387 - 2390
反应条件
indium(III) chloride in 1,2-dichloro-ethane
0.2 h; Heating;
参考文献
Ranu, Brindaban C.; Das, Arijit; Samanta, Sampak
Synlett, 2002 , # 5 p. 727 - 730
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
参考文献
Anderson,L.C.; Pinnick,H.W.
Journal of Organic Chemistry, 1978 , vol. 43, p. 3417 - 3418
反应条件
2,4,4,6-tetrabromo-2,5-cyclohexadien-1-one in chloroform
T=20°C; 0.333333 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza; Zolfigol
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 5 p. 1047 - 1071
反应条件
acetyl chloride in methanol
0.5 h; RefluxGreen chemistry; TemperatureTime; chemoselective reaction;
参考文献
Yu, Hai-Feng
Synthetic Communications, 2013 , vol. 43, # 9 p. 1280 - 1286
反应条件
1: 95 percent / hydrogen / PtO2 / ethanol; tetrahydrofuran / 5 h / 2585.7 Torr
View Scheme
参考文献
Walton, Richard; Lahti, Paul M.
Synthetic Communications, 1998 , vol. 28, # 6 p. 1087 - 1092
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=-40°C; 0.00416667 h; Inert atmosphere;
参考文献
Blazej, Sylwia; Makosza, Mieczyslaw
Chemistry - A European Journal, 2008 , vol. 14, # 35 p. 11113 - 11122
反应条件
1: NH2NH2 / Rh/C / tetrahydrofuran; H2O / 1 h
2: 60 percent / PCC / tetrahydrofuran / 0.17 h
3: 90 percent / HCl / H2O / 0.83 h
View Scheme
参考文献
Creary, Xavier; Engel, Paul S.; Kavaluskas, Natasha; Pan, Li; Wolf, Allison
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5634 - 5643