2-(4-氯苯基)-1,3-二氧戊环合成路线 （共 31 条）
反应条件
1: With naphthalene; lithium in tetrahydrofuran T=-80°C; 3 h; 2: With water in tetrahydrofuran cooling;
参考文献
Azzena, Ugo; Dettori, Giovanna; Sforazzini, Giuseppe; Yus, Miguel; Foubelo, Francisco
Tetrahedron, 2006 , vol. 62, # 7 p. 1557 - 1563
反应条件
1: With naphthalene; lithium in tetrahydrofuran T=-80°C; 3 h; 2: With water in tetrahydrofuran cooling;
参考文献
Tetrahedron, , vol. 62, # 7 p. 1557 - 1563
反应条件
caesium carbonate in 2,2,2-trifluoroethanol 15 h; Inert atmosphereIrradiation;
参考文献
Journal of Organic Chemistry, , vol. 77, # 20 p. 9094 - 9101
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI 1.) benzene/THF, 63 deg C, 1.75 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
hydrogenchloride; hydroxylamine hydrochloride 2 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 41, # 11 p. 2042 - 2043
反应条件
1: 1,1-ethylenedioxy-1-(4-chlorophenyl)methane With naphthalene; lithium in tetrahydrofuran T=-78°C; 1.5 h; Inert atmosphere; 2: N,N-dimethyl acetamide in tetrahydrofuran 2 h; Inert atmosphere; 3: With hydrogenchloride in tetrahydrofuran 1 h; Inert atmosphere;
参考文献
Martinez, Ricardo; Ramon, Diego J.; Yus, Miguel
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 9 p. 1235 - 1240
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether 12 h; Heating; Yield given. Yields of byproduct given;
参考文献
Gazzetta Chimica Italiana, , vol. 121, # 9 p. 445 - 447
反应条件
2,4,6-trichloro-1,3,5-triazine in N,N-dimethyl-formamide T=20°C; 0.583333 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Bettigeri, Sampada V.
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 67 - 71
反应条件
1: With naphthalene; lithium in tetrahydrofuran T=-80°C; 3 h; 2: With water in tetrahydrofuran cooling;
参考文献
Tetrahedron, , vol. 62, # 7 p. 1557 - 1563
反应条件
lithium aluminium tetrahydride; (η5-C5H5)titanium trichloride in diethyl ether 12 h; Heating; Title compound not separated from byproducts;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 5 p. 421 - 424
