4-(2-甲基丙-1-烯基)吗啉合成路线 （共 26 条）
参考文献
Bielitza, Max; Pietruszka, Joerg
Synlett, 2012 , vol. 23, # 11 p. 1625 - 1628
反应条件
1: 100 percent / 3 h / 60 - 70 °C 2: 1.) lithium diisopropylamide / 1.) THF, hexane, room temp., 1 h; 2.) THF, 60 deg C, 5 min View Scheme
参考文献
Knorr, Rudolf; Loew, Peter; Hassel, Petra
Synthesis, 1983 , # 10 p. 785 - 786
反应条件
lithium diisopropyl amide 1.) THF, hexane, room temp., 1 h; 2.) THF, 60 deg C, 5 min; Yield given. Multistep reaction;
参考文献
Knorr, Rudolf; Loew, Peter; Hassel, Petra
Synthesis, 1983 , # 10 p. 785 - 786
反应条件
in dichloromethane T=-20°C; KineticsEquilibrium constant; Further Variations:Temperaturesconcentrations;
参考文献
Lemek, Tadeusz; Mayr, Herbert
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 6880 - 6886
参考文献
Synthetic Communications, , vol. 31, # 23 p. 3569 - 3575
反应条件
oxygen; Cu-X zeolite in 1,2-dichloro-ethane; acetonitrile T=50°C; Oxidation; Oxidative cleavage; 5 h;
参考文献
Ebitani, Kohki; Nagashima, Kohji; Mizugaki, Tomoo; Kaneda, Kiyotomi
Chemical Communications, 2000 , # 10 p. 869 - 870
反应条件
water 1) CH2Cl2, -30 deg C, 2) chromat. on a silica gel column; Yield given. Multistep reaction;
参考文献
Rossi, E.; Stradi, R.; Benedusi, A.
Tetrahedron, 1987 , vol. 43, # 20 p. 4785 - 4792
反应条件
trifluoroacetic acid 1) CH3CN, 30 min, room temperature, 2) 2 h, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Griengl, Herfried; Prischl, Gerhard; Bleikolm, Anton
Liebigs Annalen der Chemie, 1980 , # 10 p. 1573 - 1582
反应条件
trifluoroacetic acid 1) CH3CN, 30 min, room temperature, 2) 20 h, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Griengl, Herfried; Prischl, Gerhard; Bleikolm, Anton
Liebigs Annalen der Chemie, 1980 , # 10 p. 1573 - 1582
反应条件
trifluoroacetic acid 1) THF, 30 min, room temperature, 2) 4 h, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Griengl, Herfried; Prischl, Gerhard; Bleikolm, Anton
Liebigs Annalen der Chemie, 1980 , # 10 p. 1573 - 1582
