2,3-二甲基-5-硝基萘合成路线 (共 4 条)
反应条件
dinitrogen tetraoxide in dichloromethane T=20°C; further reagent nitric acid;
参考文献
Eberson, Lennart; Radner, Finn
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 1 p. 71 - 78
反应条件
1: tetrabutylammonium hexafluorophosphate / CH2Cl2 / -70 °C / anodic oxidation 2: nitrogen dioxide / CH2Cl2 / -70 deg C -> 0 deg C View Scheme
参考文献
Eberson, Lennart; Radner, Finn
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 1 p. 71 - 78
反应条件
1: NH2OH*HCl, KOH
2: NaNO2, H2SO4
View Scheme
参考文献
Robinson,S.R.; Wells,C.H.J.
Tetrahedron, 1973 , vol. 29, p. 2203 - 2207
反应条件
hydrazine hydrate; palladium on activated charcoal
参考文献
Robinson,S.R.; Wells,C.H.J.
Tetrahedron, 1973 , vol. 29, p. 2203 - 2207