乙基2-羟基-2-苯丙酸酯合成路线 （共 4 条）
反应条件
water; potassium carbonate in ethanol 4 h; Heating; Yield given;
参考文献
Kuchar; Brunova; Rejholec; et al.
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 1 p. 122 - 136
反应条件
1: (i) NaH, DMF, (ii) /BRN= 605308/ 2: aq. NaOH / ethanol / Heating 3: (i) COCl2, Py, toluene, benzene, (ii) liq. NH3, Et2O View Scheme
参考文献
UCB
Patent: GB1113218 , 1968 ;
Chem.Abstr., 1968 , vol. 69, # 51852
反应条件
N-(1,1,2,3,3,3-hexafluoropropyl)-diethylamine in dichloromethane 24 h; Ambient temperature;
参考文献
Journal of Fluorine Chemistry, , vol. 47, # 2 p. 187 - 192
反应条件
1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere
2: 4-(N,N-dimethlyamino)pyridine; triethylamine; p-toluenesulfonyl chloride / dichloromethane / 24 h / 0 - 50 °C / Inert atmosphere
View Scheme
参考文献
Infante, Rebeca; Nieto, Javier; Andres, Celia
Chemistry - A European Journal, 2012 , vol. 18, # 14 p. 4375 - 4379
