2-氯-6-硝基苯并噻唑合成路线 （共 33 条）
反应条件
phosphorus pentachloride; trichlorophosphate
参考文献
Yakugaku Zasshi, , vol. 62, p. 47,51; dtsch. Ref. S. 19, 22
Chem.Abstr., , p. 609
反应条件
(i) KSCN, Br2, (ii) aq. NaOH, (iii) /BRN= 1098293/, (iv) SO2Cl2; Multistep reaction;
参考文献
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, , vol. 283, p. 319 - 321
参考文献
Scott; Watt
Journal of Organic Chemistry, 1937 , vol. 2, p. 148,153
反应条件
1: 99 percent / anhydrous potassium fluoride / 18-crown-6-acetonitrile complex / acetonitrile / 4 h / Heating 2: 31 percent / iron powder, acetic acid / ethanol / 3 h / Heating View Scheme
参考文献
Gallagher, Peter T.; Iddon, Brian; Suschitzky, Hans
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2358 - 2361
反应条件
ethanol; hydrazine hydrate
参考文献
Colonna; Andrisano
Pubbl. Ist. Chim. ind. Univ. Bologna, 1943 , # 6 p. 3
Full Text Show Details
Katz
Journal of the American Chemical Society, 1951 , vol. 73, p. 4007,4009
Full Text Show Details
Colonna
Gazzetta Chimica Italiana, 1948 , vol. 78, p. 462,467, 469
反应条件
1: With iron in ethanol; acetic acid 1.5 h; Heating / reflux; 2: With sodium hydroxide in ethanol; water; acetic acid pH=7.5;
参考文献
STERIX LIMITED
Patent: WO2004/37251 A1, 2004 ;
Location in patent: Page/Page column 99; 100 ;
反应条件
ammonium hydroxide T=150 - 160°C; unter Druck;
参考文献
Journal of the Indian Chemical Society, , vol. 10, p. 563,568
反应条件
1: 99 percent / anhydrous potassium fluoride / 18-crown-6-acetonitrile complex / acetonitrile / 4 h / Heating 2: 6 percent / tin, conc. hydrochloric acid / ethanol / 1 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2358 - 2361
反应条件
in tetrahydrofuran; water
参考文献
ELI LILLY AND COMPANY
Patent: WO2006/66173 A2, 2006 ;
Location in patent: Page/Page column 84 ;
WO 2006/066173 A2
参考文献
Scott; Watt
Journal of Organic Chemistry, 1937 , vol. 2, p. 148,153
