乙基6-甲基-5-氧代庚酸酯合成路线 (共 6 条)
反应条件
hydrogenchloride; sulfuric acid 12 h; Heating;
参考文献
Berthelot; Vaccher; Devergnies; Flourquet; Debaert
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 5 p. 1525 - 1529
反应条件
sodium hydride in diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 37, p. 259 - 268
反应条件
1: 28 percent / 4 N aq. NaOH, H2O2 / methanol / Ambient temperature; overnight 2: 74 percent / conc. H2SO4, HCl(g) / 12 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 25, # 5 p. 1525 - 1529
反应条件
1: 61 percent / aq. NaOH / Ambient temperature; overnight 2: 28 percent / 4 N aq. NaOH, H2O2 / methanol / Ambient temperature; overnight 3: 74 percent / conc. H2SO4, HCl(g) / 12 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 25, # 5 p. 1525 - 1529
反应条件
1: iron (III) acetylacetonate / tetrahydrofuran / 0 °C 2: sulfuric acid / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 8 p. 3647 - 3654
反应条件
sodium hydroxide; dihydrogen peroxide T=-10°C;
参考文献
Bulletin de la Societe Chimique de France, , p. 2871 - 2875