二异丙基(乙氧基羰甲基)磷酸酯合成路线 （共 16 条）
反应条件
potassium tert-butylate in tetrahydrofuran T=-78°C;
参考文献
Oi, Ryu; Sharpless, K. Barry
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2095 - 2098
反应条件
potassium tert-butylate in tetrahydrofuran T=-78°C;
参考文献
Oi, Ryu; Sharpless, K. Barry
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2095 - 2098
反应条件
1: With sodium hydride
2: With diisobutylaluminium hydride
参考文献
Storer, Richard; Moussa, Adel; Wang, Jingyang; Chaudhuri, Narayan C.; Mathieu, Steven; Stewart, Alistair
Patent: US2005/59632 A1, 2005 ;
Location in patent: Page/Page column 25 ;
参考文献
Finan, James M.; Kishi, Yoshito
Tetrahedron Letters, 1982 , vol. 23, # 27 p. 2719 - 2722
反应条件
1: diisopropyl (ethoxycarbonyl)methylphosphonate With sodium hydride in tetrahydrofuran
T=20°C; 0.5 h;
2: 3-phenyl-propionaldehyde in tetrahydrofuran
T=0°C; Wittig olefination; 1 h;
参考文献
Mordini, Alessandro; Peruzzi, Daniela; Russo, Francesco; Valacchi, Michela; Reginato, Gianna; Brandi, Alberto
Tetrahedron, 2005 , vol. 61, # 13 p. 3349 - 3360
反应条件
Multistep reaction.;
参考文献
Bower, John F.; Williams, Andrew J.; Woodward, Hannah L.; Szeto, Peter; Lawrence, Ron M.; Gallagher, Timothy
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 16 p. 2636 - 2644
