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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
24075-49-8
合成路线
（共 8 条）
683800-15-9
→
反应条件
24075-49-8
反应条件
palladium on activated charcoal
参考文献
Liu, Cong; Han, Xiaoqing; Wang, Xiang; Widenhoefer, Ross A.
Journal of the American Chemical Society, 2004 , vol. 126, # 12 p. 3700 - 3701
1305305-87-6
→
反应条件
24075-49-8
反应条件
silver hexafluoroantimonate; PPh3 gold(I) chloro complex in nitromethane T=60°C; 0.3 h; Inert atmosphere;
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
683799-95-3
→
反应条件
24075-49-8
+
683800-15-9
反应条件
hydrogenchloride; platinum (II) chloride in 1,4-dioxane T=60°C; 24 h; Product distribution; Further Variations:ReagentsTemperaturesreaction time;
参考文献
Liu, Cong; Han, Xiaoqing; Wang, Xiang; Widenhoefer, Ross A.
Journal of the American Chemical Society, 2004 , vol. 126, # 12 p. 3700 - 3701
27421-51-8
1-甲基吲哚-2-甲醛
→
反应条件
24075-49-8
反应条件
1.1: TMG / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 1.2: 5 h / 0 °C / Inert atmosphere 2.1: PPh3 gold(I) chloro complex; silver hexafluoroantimonate / nitromethane / 0.3 h / 60 °C / Inert atmosphere View Scheme
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
1477-50-5
2-吲哚甲酸
→
反应条件
24075-49-8
反应条件
1.1: sulfuric acid / 24 h / Reflux 2.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere 2.2: 0 - 20 °C / Inert atmosphere 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 4.1: manganese(IV) oxide / dichloromethane / 12 h / Reflux 5.1: TMG / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 5.2: 5 h / 0 °C / Inert atmosphere 6.1: PPh3 gold(I) chloro complex; silver hexafluoroantimonate / nitromethane / 0.3 h / 60 °C / Inert atmosphere View Scheme
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
1485-22-9
(1-甲基-1H-吲哚-2-基)-甲醇
→
反应条件
24075-49-8
反应条件
1.1: manganese(IV) oxide / dichloromethane / 12 h / Reflux 2.1: TMG / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 2.2: 5 h / 0 °C / Inert atmosphere 3.1: PPh3 gold(I) chloro complex; silver hexafluoroantimonate / nitromethane / 0.3 h / 60 °C / Inert atmosphere View Scheme
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
1202-04-6
吲哚-2-羧酸甲酯
→
反应条件
24075-49-8
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 3.1: manganese(IV) oxide / dichloromethane / 12 h / Reflux 4.1: TMG / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 4.2: 5 h / 0 °C / Inert atmosphere 5.1: PPh3 gold(I) chloro complex; silver hexafluoroantimonate / nitromethane / 0.3 h / 60 °C / Inert atmosphere View Scheme
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
37493-34-8
1-甲基-2-吲哚甲酸甲酯
→
反应条件
24075-49-8
反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 2.1: manganese(IV) oxide / dichloromethane / 12 h / Reflux 3.1: TMG / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 3.2: 5 h / 0 °C / Inert atmosphere 4.1: PPh3 gold(I) chloro complex; silver hexafluoroantimonate / nitromethane / 0.3 h / 60 °C / Inert atmosphere View Scheme
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
