2,2,6-三甲基环己酮合成路线 (共 96 条)
反应条件
aluminum oxide; silver tetrafluoroborate in dichloromethane Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 28, # 14 p. 1545 - 1548
反应条件
potassium hydride 1) Et2O, 25 deg C, 1-3 H, 2) Et2O, -30 to 25 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 16 p. 4469 - 4470
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane 78 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 7 p. 2094 - 2114
参考文献
Journal of the Chemical Society, , p. 1565,1567
参考文献
Journal of the Chemical Society, , p. 1565,1567
反应条件
potassium carbonate; acetone anschl. mit wss. NaOH;
参考文献
Journal of the Chemical Society, , p. 919
反应条件
sodium hydroxide 1) MeOH, H2O, reflux, 3 d; Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 113, # 5 p. 1907 - 1920
反应条件
(i) aq. N2H4, KOH, diethylene glycol, (heating), (ii) CrO3, aq. H2SO4, acetone; Multistep reaction;
参考文献
Tetrahedron, , vol. 30, p. 1065 - 1072
反应条件
(i) nBu3SnOMe, Et2O, (ii) nBuMgCl, (iii) /BRN= 969135/, HMPT; Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 55, p. 273 - 294
反应条件
(i) nBuMgBr, HMPT, (ii) /BRN= 609209/; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 160 - 171