1-苯基-2-(苯基甲硫基)乙酮合成路线 (共 45 条)
反应条件
triethylamine in diethyl ether
参考文献
Brown, Michael D.; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 817 - 822
反应条件
1: 85 percent / 1 h / 100 °C
2: 2percent aq. NaOH / ethanol / 10 h
View Scheme
参考文献
Singh, Harjit; Batra, Manohar S.; Singh, Paramjit
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 131 - 136
反应条件
1.1: sodium hydroxide / ethanol / 0.83 h / 25 °C
1.2: 25 °C
2.1: potassium carbonate / 20 °C
2.2: 20 °C
3.1: sodium hydroxide / ethanol / 0.83 h / 25 °C
3.2: 25 °C
View Scheme
参考文献
Yu, Haifeng
Chinese Journal of Chemistry, 2012 , vol. 30, # 2 p. 367 - 371
反应条件
1.1: sodium hydroxide / ethanol / 0.83 h / 25 °C
1.2: 25 °C
2.1: potassium carbonate / 20 °C
2.2: 20 °C
3.1: sodium hydroxide / ethanol / 0.83 h / 25 °C
3.2: 25 °C
View Scheme
参考文献
Yu, Haifeng
Chinese Journal of Chemistry, 2012 , vol. 30, # 2 p. 367 - 371
反应条件
1.1: sodium hydroxide / ethanol / 0.83 h / 25 °C
1.2: 25 °C
2.1: potassium carbonate / 20 °C
2.2: 20 °C
3.1: sodium hydroxide / ethanol / 0.83 h / 25 °C
3.2: 25 °C
View Scheme
参考文献
Yu, Haifeng
Chinese Journal of Chemistry, 2012 , vol. 30, # 2 p. 367 - 371
反应条件
1.1: potassium carbonate / 20 °C
1.2: 20 °C
2.1: sodium hydroxide / ethanol / 0.83 h / 25 °C
2.2: 25 °C
View Scheme
参考文献
Yu, Haifeng
Chinese Journal of Chemistry, 2012 , vol. 30, # 2 p. 367 - 371
反应条件
1.1: bromine / methanol / 20 °C / Cooling with ice
2.1: sodium hydroxide / methanol / 0.17 h / 20 °C
2.2: 20 °C
View Scheme
参考文献
Li, Qing-Shan; Li, Cui-Yun; Lu, Xiang; Zhang, Hui; Zhu, Hai-Liang
European Journal of Medicinal Chemistry, 2012 , vol. 50, p. 288 - 295
反应条件
sodium hydroxide in methanol
参考文献
Malashko,P.M.; Tishchenko,I.G.
Journal of Organic Chemistry USSR (English Translation), 1969 , vol. 5, p. 68 - 72
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, # 1 p. 70 - 75
反应条件
sodium hydroxide in ethanol
8 h;
参考文献
Singh, Harjit; Batra, Manohar S.; Singh, Paramjit
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 131 - 136
反应条件
sodium hydroxide in ethanol
10 h;
参考文献
Singh, Harjit; Batra, Manohar S.; Singh, Paramjit
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 131 - 136