1-苯基-2-(苯基甲硫基)乙酮合成路线 （共 45 条）
反应条件
sodium hydroxide in ethanol
参考文献
Singh, Harjit; Batra, Manohar S.; Singh, Paramjit
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 131 - 136
反应条件
sodium hydroxide in benzene
144 h;
参考文献
Singh, Harjit; Malhotra, Nageshwar; Batra, Manohar S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 272 - 273
反应条件
n-butyllithium; diisopropylamine
1.) THF, hexane, -60 deg C, 15 min, 2.) -60 deg C up to r.t.; Yield given. Multistep reaction;
参考文献
Scholz, Dieter
Monatshefte fuer Chemie, 1984 , vol. 115, p. 1121 - 1124
反应条件
in tetrahydrofuran
0.25 h; Yield given;
参考文献
Fox, Marye Anne; Triebel, Carol A.; Rogers, Ralph
Synthetic Communications, 1982 , vol. 12, # 13 p. 1055 - 1062
反应条件
in tetrahydrofuran
0.25 h; Yield given;
参考文献
Fox, Marye Anne; Triebel, Carol A.; Rogers, Ralph
Synthetic Communications, 1982 , vol. 12, # 13 p. 1055 - 1062
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; TiCpCl2; 2-methylpropylmagnesium bromide
1.) THF, 20 deg C, 1 h, 2.) THF, room temperature, 30 min; 60 deg C, 2 h; Yield givenMultistep reaction;
参考文献
Huang; Zheng
Synthetic Communications, 1999 , vol. 29, # 8 p. 1297 - 1301
参考文献
Singh, Harjit; Batra, Manohar S.; Singh, Paramjit
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 131 - 136
参考文献
Dodson
Journal of the American Chemical Society, 1948 , vol. 70, p. 2753
参考文献
Dodson
Journal of the American Chemical Society, 1948 , vol. 70, p. 2753
反应条件
1: 1.) NaH / 1.) THF, reflux, 30 m, 2.) THF, 20 deg C, 16 h
2: 1.) THF, reflux, 1 h, 2.) THF, 20 deg C, reflux, 1 h
3: 80 percent / LiBr / diethyl ether / 20 °C
4: 89 percent / sodium in ammonia, ammonium chloride / diethyl ether / 0.33 h
5: toluene-p-sulphonic acid / benzene / Heating
6: 75 percent / LDA / diethyl ether / 9 h / 20 °C
View Scheme
参考文献
Brown, Michael D.; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 817 - 822
