5-甲氧基-6-[(3-甲基-2-丁烯-1-基)氧基]-2H-呋喃并[2,3-h]-1-苯并吡喃-2-酮合成路线 （共 5 条）
反应条件
potassium carbonate in acetone 4 h;
参考文献
Reed, Michael W.; Moore, Harold W.
Journal of Organic Chemistry, 1988 , vol. 53, # 8 p. 4166 - 4171
反应条件
1: 1.) n-butyllithium / 1.) THF, -78 deg C, 5 min, 2.) -78 deg C, 15 min 2: aq. ceric ammonium nitrate (CAN), / acetonitrile / 0.25 h / 0 °C 3: H2 / 5percent Pd/CaCO3 (Pb poisoned) / tetrahydrofuran / 2 h 4: 89 percent / K2CO3 / acetone / 4 h View Scheme
参考文献
Reed, Michael W.; Moore, Harold W.
Journal of Organic Chemistry, 1988 , vol. 53, # 8 p. 4166 - 4171
反应条件
1: H2 / 5percent Pd/CaCO3 (Pb poisoned) / tetrahydrofuran / 2 h 2: 89 percent / K2CO3 / acetone / 4 h View Scheme
参考文献
Reed, Michael W.; Moore, Harold W.
Journal of Organic Chemistry, 1988 , vol. 53, # 8 p. 4166 - 4171
反应条件
1: 1.) aq. AgNO3 2.) aq. KCN / 1.) ethanol, 45 min. 2.) 1.5 h 2: 1.) n-butyllithium / 1.) THF, -78 deg C, 5 min, 2.) -78 deg C, 15 min 3: aq. ceric ammonium nitrate (CAN), / acetonitrile / 0.25 h / 0 °C 4: H2 / 5percent Pd/CaCO3 (Pb poisoned) / tetrahydrofuran / 2 h 5: 89 percent / K2CO3 / acetone / 4 h View Scheme
参考文献
Reed, Michael W.; Moore, Harold W.
Journal of Organic Chemistry, 1988 , vol. 53, # 8 p. 4166 - 4171
反应条件
1: aq. ceric ammonium nitrate (CAN), / acetonitrile / 0.25 h / 0 °C 2: H2 / 5percent Pd/CaCO3 (Pb poisoned) / tetrahydrofuran / 2 h 3: 89 percent / K2CO3 / acetone / 4 h View Scheme
参考文献
Reed, Michael W.; Moore, Harold W.
Journal of Organic Chemistry, 1988 , vol. 53, # 8 p. 4166 - 4171
