1-(甲基磺酰基)-4-哌啶羰酰氯合成路线 （共 4 条）
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane T=20°C; 3 h;
参考文献
Imamura, Shinichi; Nishikawa, Youichi; Ichikawa, Takashi; Hattori, Taeko; Matsushita, Yoshihiro; Hashiguchi, Shohei; Kanzaki, Naoyuki; Iizawa, Yuji; Baba, Masanori; Sugihara, Yoshihiro
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 2 p. 397 - 416
反应条件
in dichloromethane; N,N-dimethyl-formamide; Petroleum ether
参考文献
Takeda Chemical Industries, Ltd.
Patent: US6562978 B1, 2003 ;
反应条件
1: 92 percent / NaOH / H2O / 3 h 2: 97 percent / oxalyl chloride; DMF / CH2Cl2 / 3 h / 20 °C View Scheme
参考文献
Imamura, Shinichi; Nishikawa, Youichi; Ichikawa, Takashi; Hattori, Taeko; Matsushita, Yoshihiro; Hashiguchi, Shohei; Kanzaki, Naoyuki; Iizawa, Yuji; Baba, Masanori; Sugihara, Yoshihiro
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 2 p. 397 - 416
反应条件
1: 89 percent / triethylamine / ethyl acetate / 2.5 h / 20 °C 2: 92 percent / NaOH / H2O / 3 h 3: 97 percent / oxalyl chloride; DMF / CH2Cl2 / 3 h / 20 °C View Scheme
参考文献
Imamura, Shinichi; Nishikawa, Youichi; Ichikawa, Takashi; Hattori, Taeko; Matsushita, Yoshihiro; Hashiguchi, Shohei; Kanzaki, Naoyuki; Iizawa, Yuji; Baba, Masanori; Sugihara, Yoshihiro
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 2 p. 397 - 416
