3-(4-氯苯基)喹唑啉-4-酮合成路线 (共 24 条)
反应条件
zirconyl(IV) chloride octahydrate in ethanol; water
T=60°C; 0.5 h;
参考文献
Sangshetti, Jaiprakash N.; Kokare, Nagnnath D.; Shinde, Devanand B.
Monatshefte fur Chemie, 2007 , vol. 138, # 12 p. 1289 - 1291
反应条件
Al(NO3)3*9H2O
T=20°C; 0.233333 h; Neat (no solvent);
参考文献
Wang, Min; Song, Zhiguo; Zhang, Tingting
Synthetic Communications, 2011 , vol. 41, # 3 p. 385 - 391
反应条件
copper(l) iodide; caesium carbonate; (2S,4R)-2-carboxy-4-hydroxypyrrolidine in N,N-dimethyl-formamide
T=80°C; 24 h; Inert atmosphere;
参考文献
Xu, Lanting; Jiang, Yongwen; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 4 p. 1150 - 1153
反应条件
sodium tetrahydroborate; nickel dichloride in methanol
T=20°C; 0.5 h;
参考文献
Khurana, Jitender M.; Kukreja, Gagan
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 4 p. 677 - 679
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; di-(1-adamantyl)-n-butylphosphine in 1,4-dioxane
T=100°C; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
He, Lin; Li, Haoquan; Neumann, Helfried; Beller, Matthias; Wu, Xiao-Feng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1420 - 1424
Angew. Chem., 2014 , vol. 126, # 5 p. 1444 - 1448,5
反应条件
titanium tetrachloride; zinc in tetrahydrofuran
Heating;
参考文献
Shi, Daqing; Rong, Liangce; Wang, Juxian; Zhuang, Qiya; Wang, Xiangshan; Hu, Hongwen
Synthetic Communications, 2004 , vol. 34, # 10 p. 1759 - 1765
反应条件
iodine; orthoformic acid triethyl ester in ethanol
T=20°C; Reflux; chemoselective reaction;
参考文献
Zeng, Li-Yan; Cai, Chun
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 5 p. 1035 - 1039
反应条件
copper(l) iodide; potassium carbonate in N,N-dimethyl-formamide
T=80°C; 6 h; Inert atmosphere;
参考文献
Zhou, Jing; Fu, Liangbing; Lv, Man; Liu, Jinsong; Pei, Duanqing; Ding, Ke
Synthesis, 2008 , # 24 art. no. F18308SS, p. 3974 - 3980
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate
T=20°C; 0.166667 h; Ionic liquidSonication;
参考文献
Pawar, Omprakash B.; Chavan, Fulchand R.; Sakate, Sachin S.; Shinde, Narayan D.
Chinese Journal of Chemistry, 2010 , vol. 28, # 1 p. 69 - 71
反应条件
silicagel supported phosphomolybdic acid
T=20°C; 0.133333 h; Inert atmosphere;
参考文献
Sabitha, Gowravaram; Reddy, N. Mallikarjuna; Prasad, M. Nagendra; Raja; Yadav
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 3 p. 589 - 593