暂无反应条件数据

hydrogen; palladium on activated charcoal in ethyl acetate 24 h;

tetrabutyl ammonium fluoride in tetrahydrofuran T=25°C; 3 h;

1: 75 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 °C 2: 99 percent / toluene / 24 h / Heating 3: 93 percent / hydrogen / Pd/C / ethyl acetate / 24 h View Scheme

1: 93 percent / NaBH4; H2O / tetrahydrofuran / 0.67 h / 0 °C 2: 74 percent / sodium azide; PPh3 / CCl4; dimethylformamide / 12 h / Heating 3: 75 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 °C 4: 99 percent / toluene / 24 h / Heating 5: 93 percent / hydrogen / Pd/C / ethyl acetate / 24 h View Scheme

1: 74 percent / sodium azide; PPh3 / CCl4; dimethylformamide / 12 h / Heating 2: 75 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 °C 3: 99 percent / toluene / 24 h / Heating 4: 93 percent / hydrogen / Pd/C / ethyl acetate / 24 h View Scheme

1: 99 percent / toluene / 24 h / Heating 2: 93 percent / hydrogen / Pd/C / ethyl acetate / 24 h View Scheme

1: 74 percent / Na2CO3 / dimethylformamide / 12 h / 60 °C 2: 93 percent / NaBH4; H2O / tetrahydrofuran / 0.67 h / 0 °C 3: 74 percent / sodium azide; PPh3 / CCl4; dimethylformamide / 12 h / Heating 4: 75 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 °C 5: 99 percent / toluene / 24 h / Heating 6: 93 percent / hydrogen / Pd/C / ethyl acetate / 24 h View Scheme

1: 92 percent / imidazole / dimethylformamide / 24 h / 25 °C 2: 61 percent / H2 / 10percent Pd/C / 4 h / 2585.7 Torr 3: 89 percent / toluene / 16 h / Heating 4: 75 percent / tetrabutylammonium fluoride / tetrahydrofuran / 3 h / 25 °C View Scheme

1: 89 percent / toluene / 16 h / Heating 2: 75 percent / tetrabutylammonium fluoride / tetrahydrofuran / 3 h / 25 °C View Scheme