1-(2,4-二羟基苯基)-2-(3,4-二甲氧基苯基)乙酮合成路线 （共 9 条）
反应条件
boron trifluoride diethyl etherate T=80°C; 2 h; Inert atmosphere;
参考文献
Ng, Lean-Teik; Ko, Horng-Huey; Lu, Tzy-Ming
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 13 p. 4360 - 4366
反应条件
aluminium trichloride; nitrobenzene
参考文献
Badcock et al.
Journal of the Chemical Society, 1950 , p. 2961,2963
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Boyd; Robertson
Journal of the Chemical Society, 1948 , p. 174
反应条件
2: sodium 3: aqueous hydriodic acid; acetic acid anhydride View Scheme
参考文献
Dhar et al.
Journal of Scientific and Industrial Research, 1955 , vol. 14 B, p. 73
反应条件
boron trifluoride diethyl etherate; methanesulfonyl chloride
T=50 - 110°C; 2 h; Inert atmosphere;
参考文献
Deodhar, Mandar; Wood, Kasey; Black, David Stclair; Kumar, Naresh
Australian Journal of Chemistry, 2012 , vol. 65, # 10 p. 1377 - 1383,7
反应条件
in morpholine; N-methyl-acetamide; chloroform
参考文献
Chinoin Gyogyszer- es Vegyeszeti Termekek Gyara Rt.
Patent: US5247102 A1, 1993 ;
反应条件
1: 1-(2,4-dihydroxyphenyl)-2-(3,4-dimethoxyphenyl)ethan-1-one With boron trifluoride diethyl etherate in N,N-dimethyl-formamide
T=0°C;
2: methanesulfonyl chloride T=100°C; 2 h;
参考文献
Yadav, Dinesh K.; Gautam, Abnish K.; Kureel, Jyoti; Srivastava, Kamini; Sahai, Mahendra; Singh, Divya; Chattopadhyay, Naibedya; Maurya, Rakesh
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 2 p. 677 - 681
反应条件
hydrogenchloride; diethyl ether
Erhitzen des Reaktionsprodukts mit Wasser;
参考文献
Dhar et al.
Journal of Scientific and Industrial Research, 1955 , vol. 14 B, p. 73
反应条件
1: diethyl ether; hydrogen chloride / Erhitzen des Reaktionsprodukts mit Wasser
2: potassium carbonate; acetone
View Scheme
参考文献
Dhar et al.
Journal of Scientific and Industrial Research, 1955 , vol. 14 B, p. 73
