1: in tetrahydrofuran
T=20°C; 24 h;
2: With water-d2 in tetrahydrofuran
T=20°C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Baird, Mark S; Nizovtsev, Alexey V; Bolesov, Ivan G
Tetrahedron, 2002 , vol. 58, # 8 p. 1581 - 1593
Akhmetkhanova, F. M.; Rol'nik, L. Z.; Proskurnina, M. V.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 31 p. 567 - 571,502 - 504
chromium hexacarbonyl in dimethyl sulfoxide
T=130°C; 3 h; Inert atmosphere;
参考文献
Lin, Shaw-Tao; Lee, Chuan-Chen; Ding, Mei-Fang; Liang, David W.; Jeng, An-Ting
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 529 - 534
