1,1'-(2,3-二甲基-1,4-丁烷二基)二(3,4-二甲氧基苯)合成路线 （共 31 条）
反应条件
hydrogen; palladium 10 on activated carbon in 1-Propyl acetate T=100°C; P=5171.62 Torr; Product distribution / selectivity;
参考文献
Li, Xu; Jiang, Jian-Hong; Chen, Qingqi; Xiao, Sheng-Xiong; Li, Chuan-Hua; Gu, Hui-Wen; Zhang, Hui; Hu, Ji-Lin; Yao, Fei-Hong; Li, Qiang-Guo
European Journal of Medicinal Chemistry, 2013 , vol. 62, p. 605 - 613
反应条件
palladium 10 on activated carbon; hydrogen in 1-Propyl acetate T=100°C; P=51716.2 Torr; 3 h; PressureTime;
参考文献
European Journal of Medicinal Chemistry, , vol. 62, p. 605 - 613
反应条件
1: erythro-nordihydroguaiaretic acid With potassium carbonate in acetone T=20°C; 0.166667 h; 2: dimethyl sulfate in acetone 8 h; Reflux;
参考文献
Meyers, Ross O.; Lambert, Joshua D.; Hajicek, Nicole; Pourpak, Alan; Kalaitzis, John A.; Dorr, Robert T.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 16 p. 4752 - 4755
反应条件
hydrogen; platinum(IV) oxide in ethyl acetate 2.5 h;
参考文献
Gezginci, Mikail H; Timmermann, Barbara N
Tetrahedron Letters, 2001 , vol. 42, # 35 p. 6083 - 6085
反应条件
lithium triethylborohydride in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Dhal; Landais; Lebrun; Lenain; Robin
Tetrahedron, 1994 , vol. 50, # 4 p. 1153 - 1164
反应条件
1: 40 percent / NaH, MeOH / toluene / 0 - 20 °C 2: 73 percent / hydrogen / 10 percent palladium on charcoal / acetic acid / 4 h / Ambient temperature 3: 82 percent / CaCl2, NaBH4 / ethanol / 0.25 h / Ambient temperature 4: 98 percent / pyridine / 0.33 h / 0 °C 5: 90 percent / LiBEt3 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 50, # 4 p. 1153 - 1164
反应条件
1: 73 percent / TiCl4; Zn / tetrahydrofuran / 3 h / Heating 2: triethyl orthoformate; benzoic acid / 100 - 180 °C 3: 100 percent / H2 / PtO2 / ethyl acetate / 2.5 h View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 35 p. 6083 - 6085
反应条件
1: triethyl orthoformate; benzoic acid / 100 - 180 °C 2: 100 percent / H2 / PtO2 / ethyl acetate / 2.5 h View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 35 p. 6083 - 6085
反应条件
1: 40 percent / NaH, MeOH / toluene / 0 - 20 °C 2: 73 percent / hydrogen / 10 percent palladium on charcoal / acetic acid / 4 h / Ambient temperature 3: 82 percent / CaCl2, NaBH4 / ethanol / 0.25 h / Ambient temperature 4: 98 percent / pyridine / 0.33 h / 0 °C 5: 90 percent / LiBEt3 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 50, # 4 p. 1153 - 1164
反应条件
1: 98 percent / pyridine / 0.33 h / 0 °C 2: 90 percent / LiBEt3 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 50, # 4 p. 1153 - 1164
