manganese; bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran T=20°C;
参考文献
Barrero, Alejandro F.; Herrador, M. Mar; Del Moral, Jose F. Quilez; Arteaga, Pilar; Arteaga, Jesus F.; Piedra, Maria; Sanchez, Elena M.
Organic Letters, 2005 , vol. 7, # 12 p. 2301 - 2304
1: n-butyllithium; sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere 2: 4-(N,N-dimethlyamino)pyridine; N,N'-dimethyl-N,N'-propyleneurea; triethylamine / 3 h / -30 - 20 °C / Inert atmosphere 3: iron (III) acetylacetonate / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 0.5 h / -40 - -20 °C / Inert atmosphere 4: diisobutylaluminium hydride / toluene / 1 h / -70 °C / Inert atmosphere View Scheme
参考文献
Lupoli, Tania J.; Tsukamoto, Hirokazu; Doud, Emma H.; Wang, Tsung-Shing Andrew; Walker, Suzanne; Kahne, Daniel
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10748 - 10751
