1-(4-甲基苯基)-3-丁烯-1-醇合成路线 (共 42 条)
反应条件
1: Al-MCM-41 (Si/Al = 26) / dichloromethane / 2.5 h / 30 °C / Inert atmosphere 2: hydrogenchloride; water / methanol / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 67, # 11 p. 2081 - 2089
反应条件
in diethyl ether P=7500600 Torr; 168 h; Ambient temperature; Yield given;
参考文献
Tetrahedron, , vol. 40, # 12 p. 2239 - 2246
反应条件
1: anhydrous iron chloride; chloramine-T / dichloromethane / 20 °C / Inert atmosphere 2: indium / dichloromethane / 20 °C / Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 5 p. 695 - 700
反应条件
hydrogenchloride; benzene-1,2-diol; triethylamine 1.) 12 h, 60 deg C; 2.) Et2O, 1 h; Yield given. Multistep reaction;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 35, # 5 p. 2155 - 2157
反应条件
hydrogenchloride 1.) CHCl3, reflux, 20 h; 2.) 1 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 20 p. 1517 - 1518
反应条件
Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 55, # 8 p. 2415 - 2420
反应条件
(Ru2(η5-C5Ph4O)2(H)2(CO)4) in 1,3,5-trimethyl-benzene T=165°C; 24 h; Inert atmosphere;
参考文献
Muthaiah, Senthilkumar; Hong, Soon Hyeok
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 3045 - 3053
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in water T=90 - 100°C; 2.5 h; var. educt/reagent ratio; Product distribution;
参考文献
Li, Chao-Jun; Wang, Dong; Chen, Dong-Li
Journal of the American Chemical Society, 1995 , vol. 117, # 51 p. 12867 - 12868
参考文献
Tetrahedron, , vol. 40, # 7 p. 1167 - 1178
反应条件
in pyridine
36 h; Ambient temperature;
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610