1-(3-甲氧基苯基)-3-丁烯-1-醇合成路线 (共 13 条)
反应条件
in pyridine 36 h; Ambient temperature;
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
1: With SnCl2·2H2O; aluminium in tetrahydrofuran
T=20°C; 0.0833333 h;
2: With water in tetrahydrofuran
T=15°C; 0.25 h;
参考文献
Vilanova, Conxin; Sanchez-Peris, Maria; Roldan, Steven; Dhotare, Bhaskar; Carda, Miguel; Chattopadhyay, Angshuman
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6562 - 6567
反应条件
Amberlyst A-15 in dichloromethane; water
T=25°C; 0.333333 h; Green chemistry;
参考文献
Couto, Tulio R.; Freitas, Juliano C.R.; Cavalcanti, Italo H.; Oliveira, Roberta A.; Menezes, Paulo H.
Tetrahedron, 2013 , vol. 69, # 34 p. 7006 - 7010
反应条件
MABR in dichloromethane
T=-20°C; 0.75 h;
参考文献
Li, Gui-Long; Zhao, Gang
Organic Letters, 2006 , vol. 8, # 4 p. 633 - 636
反应条件
ruthenium trichloride; carbon monoxide; triethylamine in 1,4-dioxane; water
T=80°C; P=1551.49 Torr; 24 h;
参考文献
Denmark, Scott E.; Nguyen, Son T.
Organic Letters, 2009 , vol. 11, # 3 p. 781 - 784
反应条件
in tetrahydrofuran
2.5 h; Ambient temperature;
参考文献
Flynn, Daniel L.; Crich, Joyce Z.; Devraj, Rajesh V.; Hockerman, Susan L.; Parlow, John J.; South, Michael S.; Woodard, Scott
Journal of the American Chemical Society, 1997 , vol. 119, # 21 p. 4874 - 4881
反应条件
1: With iron(III) chloride in nitromethane
T=-20°C; 0.5 h;
2: With hydrogenchloride
T=20°C; 0.5 h;
参考文献
Watahiki, Tsutomu; Oriyama, Takeshi
Tetrahedron Letters, 2002 , vol. 43, # 49 p. 8959 - 8962
反应条件
1: 3-methoxy-benzaldehyde With chloro-trimethyl-silane; samarium diiodide; nBu4NPF6 in tetrahydrofuran
T=20°C; Barbier Coupling Reaction; Electrochemical reaction;
2: 3-iodoprop-1-ene in tetrahydrofuran
T=20°C;
3: Acidic conditions;
参考文献
Sun, Linhao; Sahloul, Kamar; Mellah, Mohamed
ACS Catalysis, 2013 , vol. 3, # 11 p. 2568 - 2573
反应条件
in tetrahydrofuran
T=0 - 20°C;
参考文献
Lee, Sun-Mi; Lee, Won-Gil; Kim, Young-Chul; Ko, Hyojin
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 19 p. 5726 - 5729
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane
14 h; Ambient temperature; Yields of byproduct given;
参考文献
Aggarwal, Varinder K.; Vennall, Graham P.
Synthesis, 1998 , # 12 p. 1822 - 1826