1-(2-氯苯基)-3-丁烯-1-醇合成路线 （共 19 条）
反应条件
in tetrahydrofuran; diethyl ether T=0 - 20°C; 0.5 h; Inert atmosphere;
参考文献
Zhuo, Lian-Gang; Yao, Zhong-Ke; Yu, Zhi-Xiang
Organic Letters, 2013 , vol. 15, # 18 p. 4634 - 4637
反应条件
titanium(IV) isopropylate in isopropyl alcohol Meerwein-Ponndorf-Verley-Oppenauer reaction; 0.25 h; Inert atmosphereMicrowave irradiation;
参考文献
Liu, Guohua; Gao, Yan; Lu, Xiaoquan; Liu, Mouming; Zhang, Fang; Li, Hexing
Chemical Communications, 2008 , # 27 p. 3184 - 3186
反应条件
in diethyl ether T=0°C;
参考文献
Cui, Yong-Mei; Huang, Qing-Qing; Xu, Jie; Chen, Ling-Ling; Li, Jing-Ya; Ye, Qi-Zhuang; Li, Jia; Nan, Fa-Jun
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 18 p. 4130 - 4135
反应条件
1: Al-MCM-41 (Si/Al = 26) / dichloromethane / 0.5 h / 30 °C / Inert atmosphere 2: hydrogenchloride; water / methanol / 20 °C View Scheme
参考文献
Ito, Suguru; Hayashi, Akira; Komai, Hirotomo; Yamaguchi, Hitoshi; Kubota, Yoshihiro; Asami, Masatoshi
Tetrahedron, 2011 , vol. 67, # 11 p. 2081 - 2089
反应条件
ammonium chloride; magnesium 12 h; Ambient temperature;
参考文献
Zhang, Wen-Chun; Li, Chao-Jun
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3230 - 3236
反应条件
1: anhydrous iron chloride; chloramine-T / dichloromethane / 20 °C / Inert atmosphere 2: indium / dichloromethane / 20 °C / Inert atmosphere View Scheme
参考文献
Srivastava, Vishnu P.; Patel, Rajesh; Yadav, Lal Dhar S.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 695 - 700
反应条件
in N,N-dimethyl-formamide
T=150°C; 16 h;
参考文献
COUNCIL OF SCIENTIFIC and INDUSTRIAL RESEARCH; REDDY, Santhosh, Rekula; PRAGATI, Kishore, Prasad; NAGA, Kiran, Chaithanya, Indukuru; SUDALAI, Arumugam
Patent: WO2013/102935 A2, 2013 ;
Location in patent: Page/Page column 12 ;
反应条件
phenanthrene; N(Et)4ClO4 in N,N-dimethyl-formamide
T=0°C; Electrochemical reaction;
参考文献
Kurono, Nobuhito; Honda, Eiichi; Komatsu, Fumikazu; Orito, Kazuhiko; Tokuda, Masao
Chemistry Letters, 2003 , vol. 32, # 8 p. 720 - 721
反应条件
phenanthrene; N(Et)4ClO4; magnesium in N,N-dimethyl-formamide
T=0°C; Electrolysis;
参考文献
Kurono, Nobuhito; Honda, Eiichi; Komatsu, Fumikazu; Orito, Kazuhiko; Tokuda, Masao
Tetrahedron, 2004 , vol. 60, # 8 p. 1791 - 1801
