4-氰基-N,N-二甲基苯胺合成路线 (共 12 条)
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water T=90°C; 24 h;
参考文献
Liu, Zhaojun; Zhang, Jie; Chen, Shulin; Shi, Erbo; Xu, Yuan; Wan, Xiaobing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3231 - 3235
反应条件
in dichloromethane; water Inert atmosphere;
参考文献
Hanada, Shiori; Tsutsumi, Emi; Motoyama, Yukihiro; Nagashima, Hideo
Journal of the American Chemical Society, 2009 , vol. 131, # 41 p. 15032 - 15040
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Sunada, Yusuke; Kawakami, Hiroko; Imaoka, Tsuyoshi; Motoyama, Yukihiro; Nagashima, Hideo
Angewandte Chemie - International Edition, 2009 , vol. 48, # 50 p. 9511 - 9514
反应条件
tert.-butylhydroperoxide; CuO in water T=85°C; 15 h;
参考文献
Priyadarshini; Amal Joseph; Lakshmi Kantam
RSC Advances, 2013 , vol. 3, # 40 p. 18283 - 18287
反应条件
iodine; potassium carbonate in tetrachloromethane; water T=20°C; Inert atmosphere;
参考文献
Baba, Haruka; Moriyama, Katsuhiko; Togo, Hideo
Synlett, 2012 , vol. 23, # 8 p. 1175 - 1180
反应条件
1: With palladium diacetate T=20°C; 0.166667 h; Inert atmosphere; 2: With trichlorophosphate T=140°C; 60 h; Inert atmospheresealed tube;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Motevalli, Somayeh
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 355, p. 69 - 74
反应条件
1: With palladium diacetate T=20°C; 0.166667 h; Inert atmosphere; 2: With trichlorophosphate T=140°C; 15 h; Inert atmospheresealed tube;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Motevalli, Somayeh
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 355, p. 69 - 74
反应条件
tert.-butylhydroperoxide; iodine; sodium hydroxide T=70 - 80°C; 24 h;
参考文献
Xu, Kun; Hu, Yanbin; Zhang, Sheng; Zha, Zhenggen; Wang, Zhiyong
Chemistry - A European Journal, 2012 , vol. 18, # 32 p. 9793 - 9797
反应条件
1,1'-carbonyldiimidazole T=160 - 165°C; 1 h;
参考文献
Aavula, Sanjeev Kumar; Chikkulapally, Anil; Hanumanthappa; Jyothi, Indira; Vinod; Sulur, Kumar; Manjunatha; Sythana, Suresh Kumar
Journal of Chemical Research, 2013 , vol. 37, # 3 p. 155 - 159
反应条件
tert.-butylhydroperoxide; CuO in water Mechanism;
参考文献
Priyadarshini; Amal Joseph; Lakshmi Kantam
RSC Advances, 2013 , vol. 3, # 40 p. 18283 - 18287
反应条件
polymethylhydrosiloxane; HPtCl6·6H2O in tetrahydrofuran T=70°C; 4 h; Inert atmosphere; chemoselective reaction;
参考文献
Hanada, Shiori; Tsutsumi, Emi; Motoyama, Yukihiro; Nagashima, Hideo
Journal of the American Chemical Society, 2009 , vol. 131, # 41 p. 15032 - 15040