4-氟-N,N-二甲基苯甲酰胺合成路线 （共 12 条）
反应条件
LDBMOA in tetrahydrofuran; hexane T=0°C; 0.5 h;
参考文献
Kim, Yu Ri; An, Duk Keun
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 12 p. 4194 - 4196
反应条件
sodium iodide in dimethyl sulfoxide
T=20°C; Electrochemical reaction;
参考文献
Huang, Haolai; Yuan, Gaoqing; Li, Xianwei; Jiang, Huanfeng
Tetrahedron Letters, 2013 , vol. 54, # 52 p. 7156 - 7159
反应条件
tert.-butylhydroperoxide in acetonitrile
T=80°C; 24 h;
参考文献
Ekoue-Kovi, Kekeli; Wolf, Christian
Organic Letters, 2007 , vol. 9, # 17 p. 3429 - 3432
反应条件
bis(di-tert-butylphosphinous acid)PdCl2 in acetonitrile
T=50°C; 24 h;
参考文献
Ekoue-Kovi, Kekeli; Wolf, Christian
Organic Letters, 2007 , vol. 9, # 17 p. 3429 - 3432
反应条件
potassium fluoride; C94H134O4P2Pd2; silver fluoride in cyclohexane
T=90°C; 14 h; Sealed tube;
参考文献
Lee, Hong Geun; Milner, Phillip J.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2014 , vol. 136, # 10 p. 3792 - 3795
反应条件
hydrogenchloride; tert.-butylhydroperoxide; iodine in cyclohexane; water
T=70 - 80°C; 20 h;
参考文献
Gao, Lingfeng; Tang, Haoming; Wang, Zhiyong
Chemical Communications, 2014 , vol. 50, # 31 p. 4085 - 4088
反应条件
1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate in tetrachloromethane; water
T=20°C; Inert atmosphere;
参考文献
Baba, Haruka; Moriyama, Katsuhiko; Togo, Hideo
Synlett, 2012 , vol. 23, # 8 p. 1175 - 1180
反应条件
tert.-butylhydroperoxide; Cu(ClO4)2*6H2O
T=100°C; 6 h;
参考文献
Kumar, P. Santhosh; Kumar, G. Sathish; Kumar, R. Arun; Reddy, N. Veera; Rajender Reddy
European Journal of Organic Chemistry, 2013 , # 7 p. 1218 - 1222
反应条件
tert.-butylhydroperoxide; iodine; sodium hydroxide
T=70 - 80°C; 24 h;
参考文献
Xu, Kun; Hu, Yanbin; Zhang, Sheng; Zha, Zhenggen; Wang, Zhiyong
Chemistry - A European Journal, 2012 , vol. 18, # 32 p. 9793 - 9797
反应条件
1-fluoro-2,4,6-trimethylpyridinium hexafluorophosphate; C10H18CuN2(1+)*CF3O3S(1-); silver fluoride in tetrahydrofuran
T=60°C; 18 h; Inert atmosphere;
参考文献
Fier, Patrick S.; Luo, Jingwei; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 7 p. 2552 - 2559
