5-甲基嘧啶-2,4,6(1H,3H,5H)-三酮合成路线 （共 34 条）
反应条件
phosphoric acid; trichlorophosphate T=100°C; 0.75 h;
参考文献
Organic Letters, , vol. 9, # 9 p. 1639 - 1641
反应条件
1.1: N-benzyl-N,N,N-triethylammonium chloride; trichlorophosphate / 7 h / 50 °C / Inert atmosphere 2.1: N,O-bis-(trimethylsilyl)-acetamide / dichloromethane / 0.5 h / 20 °C 2.2: 0 - 20 °C 3.1: sodium tetrahydroborate / methanol / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Puig-De-La-Bellacasa, Raimon; Gimenez, Laura; Pettersson, Sofia; Pascual, Rosalia; Gonzalo, Encarna; Este, Jose A.; Clotet, Bonaventura; Borrell, Jose I.; Teixido, Jordi
European Journal of Medicinal Chemistry, 2012 , vol. 54, p. 159 - 174
参考文献
Fahr, Egon; Fecher, Peter; Roth, Georg; Wuestenfeld, Peter
Angewandte Chemie, 1980 , vol. 92, # 10 p. 858 - 859
反应条件
N-fluorobislt;(trifluoromethyl)sulfonylgt;imide in acetic acid
Ambient temperature;
参考文献
Resnati, Giuseppe; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1992 , vol. 57, # 15 p. 4281 - 4284
