in tetrahydrofuran; diethyl ether
byproducts: LiCl; N2-atmosphere; dropwise addn. of p-CH3C6H4Li in Et2O to Ru-complex in THF (molar ratio=1:1, -78°C), warming to room temp.; solvent removal (vac.), chromy. (SiO2, pentane/CH2Cl2);
参考文献
Herberhold, Max; Feger, Wolfgang; Koelle, Ulrich
Journal of Organometallic Chemistry, 1992 , vol. 436, # 3 p. 333 - 350
Wittig, G.; Maercker, A.
Journal of Organometallic Chemistry, 1967 , vol. 8, p. 491 - 494
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Gmelin Handbook: Bi: Org.Verb., 1.3.3.2.4.3, page 72 - 78
