L-谷氨酸-5-叔丁基酯合成路线 （共 17 条）
反应条件
hydrogen; palladium on activated charcoal in methanol P=760 Torr; 24 h;
参考文献
Betschmann, Patrick; Sahli, Stefan; Diederich, Francois; Obst, Ulrike; Gramlich, Volker
Helvetica Chimica Acta, 2002 , vol. 85, # 5 p. 1210 - 1245
反应条件
piperidine in N,N-dimethyl-formamide 0.5 h;
参考文献
WO2011/19942 A2, ;
Page/Page column 31-32 ;
反应条件
1: With sodium azide in N,N-dimethyl-formamide T=50°C; 4 h; 2: With piperidine in N,N-dimethyl-formamide
参考文献
Chen, Chun-Chi; Rajagopal, Basker; Liu, Xuan Yu; Chen, Kuan Lin; Tyan, Yu-Chang; Lin, Fui; Lin, Po-Chiao
Amino Acids, 2014 , vol. 46, # 2 p. 367 - 374
反应条件
sodium hydroxide in methanol T=20°C; 1.5 h; Enzymatic reaction;
参考文献
Ager, David J.; Babler, Scott; Erickson, Robert A.; Froen, Diane E.; Kittleson, Jeannine; Pantaleone, David P.; Prakash, Indra; Zhi, Ben
Organic Process Research and Development, 2004 , vol. 8, # 1 p. 72 - 85
参考文献
Justus Liebigs Annalen der Chemie, , vol. 673, p. 196 - 207
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Journal of Organic Chemistry, , vol. 28, p. 1251 - 1253
反应条件
1: H2SO4 / dioxane 2: H2 / Pd-C / aq. ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 28, p. 1251 - 1253
反应条件
hydrogenchloride; water; sodium acetate pH=4.7 - 5.0; 20 - 24 h; Conversion of starting material;
参考文献
US2004/30177 A1, ;
Page 3 ;
反应条件
water; sodium acetate T=50°C; pH=4.9; 25 h; Conversion of starting material;
参考文献
US2004/30177 A1, ;
Page 3 ;
反应条件
1: aq. NaOH 2: H2 / Pd View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 673, p. 196 - 207
