1,4,8,11-四硫杂环十四烷合成路线 (共 5 条)
反应条件
caesium carbonate in N,N-dimethyl-formamide T=45 - 50°C;
参考文献
Buter, J.; Kellogg, Richard M.
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4481 - 4485
反应条件
potassium carbonate in N,N-dimethyl-formamide T=150°C;
参考文献
Tetrahedron Letters, , vol. 46, # 46 p. 8057 - 8060
反应条件
1: thioacetimidic acid 3-acetimidoylsulfanyl-propyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT With sodium hydroxide; tetrabutylammomium bromide in benzene T=60 - 65°C; 1 h; 2: ethylene dibromide in benzene T=60 - 65°C; 1 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 178, # 6 p. 1295 - 1301
反应条件
ethanol; sodium ethanolate anschliessendes Erwaermen mit 1,3-Dibrom-propan;
参考文献
Journal of the American Chemical Society, , vol. 55, p. 780
反应条件
in CD3NO2 at room temp.; detected by NMR;
参考文献
Journal of the American Chemical Society, , vol. 113, # 23 p. 8663 - 8671