甲基N-[(苄氧基)羰基]-L-缬氨酸酯合成路线 （共 35 条）
反应条件
1: 65 percent / p-TsOH / toluene / 100 °C
2: NaHCO3 / methanol; H2O / Heating
3: H2 / Pd/C / methanol / 12 h / 20 °C
4: HCl / 12 h / 20 °C
5: CF3CO2H / 2 h / 20 °C
View Scheme
参考文献
Allevi, Pietro; Anastasia, Mario
Tetrahedron Letters, 2003 , vol. 44, # 41 p. 7663 - 7665
反应条件
sodium tetrahydroborate; lithium chloride in tetrahydrofuran; ethanol
参考文献
Higashiura, Kunihiko; Ienaga, Kazuharu
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 764 - 766
反应条件
TiCl2(OPri)2; diisobutylaluminium hydride
1.) CH2Cl2, toluene, -78 deg C, 2 h, 2.) CH2Cl2, -78 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Kiyooka; Suzuki; Shirouchi; Kaneko; Tanimori
Tetrahedron Letters, 1993 , vol. 34, # 36 p. 5729 - 5732
反应条件
TiCl2(OPri)2; diisobutylaluminium hydride
1.) CH2Cl2, toluene, -78 deg C; Yield given. Multistep reaction;
参考文献
Kiyooka; Suzuki; Shirouchi; Kaneko; Tanimori
Tetrahedron Letters, 1993 , vol. 34, # 36 p. 5729 - 5732
反应条件
TiCl2(OPri)2; diisobutylaluminium hydride
1.) CH2Cl2, toluene, -78 deg C, 2 h, 2.) CH2Cl2, -78 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Kiyooka; Suzuki; Shirouchi; Kaneko; Tanimori
Tetrahedron Letters, 1993 , vol. 34, # 36 p. 5729 - 5732
