反应条件
1: NaBH4 / ethanol / 5 h / 20 °C 2: 77 percent / DMAP / CH2Cl2 / 2 h / 20 °C 3: 83 percent / Bu3SnH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene / 2 h / Heating 4: NaOMe / methanol / 24 h / 100 °C 5: 8 mg / PTSA / dioxane; H2O / 24 h / 120 °C View Scheme
参考文献
Cassayare, Jerome; Zard, Samir Z.
Journal of the American Chemical Society, 1999 , vol. 121, # 25 p. 6072 - 6073