反应条件
1.1: hydrogen; hydrogenchloride; 5 palladium on charcoal / ethanol; ethyl acetate / 24 h / 20 °C / 760.05 Torr / |Schlenk technique 2.1: triethylamine / dichloromethane / 5 h / 20 °C 3.1: sodium hydride / toluene; mineral oil / 0.25 h / 0 °C / |Inert atmosphere 3.2: 8 h / 130 °C / |Inert atmosphere; |Dean-Stark View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 13 p. 3685 - 3689
Angew. Chem., , vol. 125, # 13 p. 3773 - 3777,5
