N,N-二乙基苯并[d]噻唑-2-胺合成路线 （共 8 条）
反应条件
1: diethylamine With copper(l) iodide 0.5 h; 2: With potassium hydroxide in water 1 h; 3: 2-chloro-1,3-benzothiazole With benzyl-tri-(n-butyl)-ammonium bromide in chloroform; water T=20°C; 6 h; chemoselective reaction;
参考文献
Verma, Sanjeev K.; Acharya; Kaushik
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 5 p. 1324 - 1327
反应条件
1,10-phenanthroline; copper diacetate; lithium tert-butylate in 1,4-dioxane T=20°C; 4 h; Inert atmosphere;
参考文献
Matsuda, Naoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Synthesis (Germany), 2012 , vol. 44, # 12 art. no. Z003111SS, p. 1792 - 1797
反应条件
pyridine; anhydrous iron chloride; sodium peroxodisulphate in dimethyl sulfoxide T=80°C; 3 h; Inert atmosphere;
参考文献
Wang, Haibo; Wang, Lu; Shang, Jinsai; Li, Xing; Wang, Haoyuan; Gui, Jie; Lei, Aiwen
Chemical Communications, 2012 , vol. 48, # 1 p. 76 - 78
反应条件
caesium carbonate in 1,4-dioxane T=130°C; 2 h;
参考文献
Journal of Combinatorial Chemistry, , vol. 12, # 4 p. 422 - 429
反应条件
potassium carbonate in water T=100°C; 5 h; Green chemistry;
参考文献
Green Chemistry, , vol. 14, # 9 p. 2491 - 2498
反应条件
T=100°C; P=6000480 Torr; 96 h; other aromatic and heteroaromatic halides; other tertiary (trialkyl and monocyclic) amines; Product distribution;
参考文献
Matsumoto, Kiyoshi; Hashimoto, Shiro; Otani, Shinichi
Journal of the Chemical Society, Chemical Communications, 1991 , # 5 p. 306 - 307
反应条件
1: neat (no solvent) 2: potassium carbonate / water / 5 h / 100 °C / |Green chemistry View Scheme
参考文献
Green Chemistry, , vol. 14, # 9 p. 2491 - 2498
反应条件
1: triethylamine / dichloromethane / 0.17 h / 20 °C / |Inert atmosphere 2: 2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane / toluene / 0.23 h / 110 °C / |Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 79, # 1 p. 251 - 266
